A Concise Practical Book on PHARMACEUTICAL ORGANIC CHEMISTRY 2 – As Per PCI Regulations For Second Year BPharm – Semester 3 | Dr Manoj Damale | Nirali Prakashan

General introduction to purification technique for crude solid: Recrystallisation
1. Recrystallization of crude acetanilide
2. Introduction to steam distillation
3. Determination of acid value of given sample
4. Determination of saponification value of given sample
5. Determination of iodine value of given sample
6. Synthesis or preparation of benzanilide from aniline (Benzoylation reaction)
7. Synthesis or preparation of 2,4,6-tribromoaniline from aniline (Bromination reaction)
8. Synthesis or preparation of para-bromoacetanilide from acetanilide (Bromination reaction)
9. Synthesis or preparation of meta-dinitrobenzene from nitrobenzene
10. Synthesis or preparation of benzoic acid from benzyl chloride (Oxidation reaction)
11. Synthesis or preparation of benzoic acid from ethyl benzoate (Alkaline hydrolysis)
12. Synthesis or preparation of 1-phenyl-azo-2-naphthol from aniline (Diazotization reaction)
13. Synthesis or preparation of benzyl from benzoin (Oxidation reaction)
14. Synthesis or preparation of dibenzalacetone from benzaldehyde (Claisen Schmidt reaction)
15. Synthesis or preparation of Cinnamic acid from benzaldehyde (Perkin’s condensation)
16. Synthesis or preparation of P-iodo benzoic acid from p-amino benzoic acid (Diazotization reaction)
Method of Preparation of Some Common Reagents
Some Common Terms used in Pharmaceutical Organic Chemistry
Examples of Common Laboratory Chemicals and their Hazard Class
Common Laboratory Techniques used in Pharmacy